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1 article(s) from Iniesta, Jesús

An alternative to hydrogenation processes. Electrocatalytic hydrogenation of benzophenone

Cristina Mozo Mulero,
Alfonso Sáez,
Jesús Iniesta and
Vicente Montiel

Beilstein J. Org. Chem. 2018, 14, 537–546, doi:10.3762/bjoc.14.40

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Graphical Abstract

Figure 1: Characterisation of Pd/C electrocatalyst. a) TEM micrograph. b) Energy dispersive X-ray analysis (E...

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Figure 2: SEM images of (a) Pd_0.02/C/T and (b) Pd_0.20/C/T electrodes, with different magnifications.

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Figure 3: Cyclic voltammetric behaviour of Pd_0.20/C/T electrode in 0.5 M H₂SO₄. Scan rate: 50 mV s⁻¹. Startin...

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Figure 4: Scheme of all components of the electrochemical reactor including reactions involved in both anode ...

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Figure 5: Fractional conversion of benzophenone as a function of coulombic passed charge using the PEMER; 0.5...

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Figure 6: Plot of cell voltage versus time obtained from a preparative electrosynthesis performed at 10 mA cm...

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Figure 7: Fractional conversion of benzophenone as a function of coulombic charge passed; 0.5 M benzophenone ...

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Figure 8: Comparison of fractional conversion (X_R) and product yield (η) between Pd_0.02/C/T, Pd_0.20/C/T and Pd...

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Figure 9: Fractional conversions of benzophenone and product yield of diphenylmethanol at both electrodes. (a...

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Figure 10: (a) General scheme of a PEMER; (b) itemisation of the main parts of PEMER: 1) endplates, 2) gas dif...

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Published 01 Mar 2018

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